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What is Solid Phase Sintering of SiC Ceramics?
Solid-phase sintering means that the sintering aid does not produce a liquid phase during the sintering of SiC ceramics, but reacts in a solid state to densify the material. In 1975, Proehazka took the lead in using a small amount of B and C force sintering aids to successfully sinter SiC ceramics without any external pressure. The addition of B and C can significantly improve the sintering kinetics of Sic. And the sintering mechanism of Sic ceramics has been studied deeply. W. Baer et al. used Al and C as sintering aids to achieve success in pressureless sintering of SiC. After that, researchers chose Al-BC series additives to sinter sic ceramics. Wu Anhua et al. used a-SiC powder as the starting material, B and C powder as sintering aids, and adopted an appropriate hot-press sintering process to prepare a-SiC block with a relative density of 97.8% at 1950C and 25MPa. The flexural strength and fracture toughness of bulk ceramics are 383MPa and 4.95MPa.m, respectively. .JJCao et al . used Al-BC series sintering aids to sinter sic ceramics at 190C and under the conditions of 190C. The density is 3.18g/cm3, the fracture toughness is as high as 9. 5MP m1/2, and the sintered body has good performance. The point of the solid phase is to require a relatively low sintering temperature (greater than 2000C) to require a higher purity of the original powder material. The sintered body has low fracture toughness and strong crack strength sensitivity. It is structurally expressed as The crystal grains are coarse and have poor uniformity, and the fracture mode is crystal fracture.
The following is SiC solid phase sintering made by SIMUWU equipment
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